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DEVELOPMENT OF AN LC/MS/MS METHOD FOR DETERMINATION ENROFLOXACIN AND CIPROFLOXACIN RESIDUES IN POULTRY MEAT
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Abstract
In this study, we developed a rapid and accurate quantitative analysis of Enrofloxacin and Ciprofloxacin residues in poultry meat by UPLC-MS/MS. Conditions of mass spectrometry include chromatographic column: C18; 100 × 2,1mm; 1.7µm, mobile phase: ACN (0.1% Formic Acid): 0.1% Formic Acid in water (80:20), flow rate: 0.3mL/min, injection volume: 2µL. Our method presented satisfactory results in terms of sensitivity, precision, accuracy, and recovery of quantitatively analyzing simultaneous Enrofloxacin and Ciprofloxacin residues in poultry meat. This method has been proved to be fast, reliable and reproducible to accurately analyze Enrofloxacin and Ciprofloxacin.
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Keywords
Enrofloxacin, Ciprofloxacin, LC/MS/MS, poultry
References
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